食欲控制補(bǔ)充劑分析
appetite suppressants by lc-ms
conditions
column: ace excel 2 superc18
dimensions: 100 x 2.1 mm
part number: exl-1011-1002u
mobile phase:
a: 10 mm ammonium acetate ph 9.35 with ammonium hydroxide
b: 10 mm ammonium acetate ph 9.35/mecn (10:90 v/v)
time(mins)
%b
0.0
11.11
1.0
11.11
21.0
100.00
23.0
100.00
flow rate: 0.5 ml/min
injection: 2 μl
temperature: 25 °c
detection: ms
1. caffeine
2. ephedrine
3. phentermine
4. phenolphthalein
5. chlordiazepoxide
6. lorcaserin
7. fenfluramine
8. fluoxetine
9. diethylpropion
10. sertraline
11. didesmethylsibutramine
12. rimonabant
13. n-desmethylsibutramine
14. sibutramine
15. orlistat